Crystallography Open Database

Information card for entry 4339752

Preview

Coordinates	4339752.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	technetium-fluoride-trioxide*technetium-trifluoride-dioxide
Chemical name	technetium-fluoride-trioxide*technetium-trifluoride-dioxide
Formula	F4 O5 Tc2
Calculated formula	F4 O5 Tc2
Title of publication	Technetium fluoride trioxide, TcO3F, preparation and properties.
Authors of publication	Supeł, Joanna; Abram, Ulrich; Hagenbach, Adelheid; Seppelt, Konrad
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	14
Pages of publication	5591 - 5595
a	8.201 ± 0.002 Å
b	14.583 ± 0.004 Å
c	5.3049 ± 0.0016 Å
α	90°
β	90.13 ± 0.011°
γ	90°
Cell volume	634.4 ± 0.3 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	20 K
Number of distinct elements	3
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0502
Residual factor for significantly intense reflections	0.0453
Weighted residual factors for significantly intense reflections	0.0941
Weighted residual factors for all reflections included in the refinement	0.0957
Goodness-of-fit parameter for all reflections included in the refinement	1.202
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179500 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/97.	4339752.cif
117517	2014-06-15	cif/ Adding structures of 4339752 via cif-deposit CGI script.	4339752.cif