Crystallography Open Database

Information card for entry 4341712

Preview

Coordinates	4341712.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32.5 O40 Si W12
Calculated formula	C32.64 O40 Si W12
Title of publication	Synthesis and Characterization of the Platinum-Substituted Keggin Anion α-H2SiPtW11O40(4-)
Authors of publication	Klonowski, Peter; Goloboy, James C.; Uribe-Romo, Fernando J; Sun, Furong; Zhu, Lingyang; Gándara, Felipe; Wills, Corinne; Errington, R. John; Yaghi, Omar M.; Klemperer, Walter G.
Journal of publication	Inorganic chemistry
Year of publication	2014
Pages of publication	141119142641005
a	17.576 ± 0.004 Å
b	17.576 ± 0.004 Å
c	17.576 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	5430 ± 2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	229
Hermann-Mauguin space group symbol	I m -3 m
Hall space group symbol	-I 4 2 3
Residual factor for all reflections	0.1091
Residual factor for significantly intense reflections	0.1036
Weighted residual factors for significantly intense reflections	0.2199
Weighted residual factors for all reflections included in the refinement	0.2222
Goodness-of-fit parameter for all reflections included in the refinement	1.176
Diffraction radiation wavelength	0.7749 Å
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4341712.cif
127638	2014-11-21	cif/ Adding structures of 4341712 via cif-deposit CGI script.	4341712.cif