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Information card for entry 4350619
Preview
| Coordinates | 4350619.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C32 H54 N4 Sb2 |
|---|---|
| Calculated formula | C32 H54 N4 Sb2 |
| Title of publication | Bis(1 degree-amino)cyclodistib(III)azanes: the first structural characterization of cis and trans isomers of a single cyclodipnict(III)azane. |
| Authors of publication | Eisler, Dana J.; Chivers, Tristram |
| Journal of publication | Inorganic chemistry |
| Year of publication | 2006 |
| Journal volume | 45 |
| Journal issue | 26 |
| Pages of publication | 10734 - 10742 |
| a | 9.955 ± 0.002 Å |
| b | 11.433 ± 0.002 Å |
| c | 31.723 ± 0.006 Å |
| α | 90° |
| β | 95.71 ± 0.03° |
| γ | 90° |
| Cell volume | 3592.7 ± 1.2 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0581 |
| Residual factor for significantly intense reflections | 0.0338 |
| Weighted residual factors for significantly intense reflections | 0.0661 |
| Weighted residual factors for all reflections included in the refinement | 0.0742 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.041 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 239969 (current) | 2019-11-25 | cif/ Adding structures of 4350618, 4350619, 4350620, 4350621, 4350622, 4350623, 4350624 via cif-deposit CGI script. |
4350619.cif |
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Users of the data should acknowledge the original authors of the
structural data.