Crystallography Open Database

Information card for entry 4503109

Preview

Coordinates	4503109.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H70 Cl8 O2 P4 Rh2
Calculated formula	C65 H70 Cl8 O2 P4 Rh2
Title of publication	Synthesis and Solid-State Behavior of Host‒Guest Carbonyl Rh(I) Polymers Assembled through Bidentate Phosphine Ligands
Authors of publication	Janjic, Nikolina; Peli, Giulia; Garlaschelli, Luigi; Sironi, Angelo; Macchi, Piero
Journal of publication	Crystal Growth & Design
Year of publication	2008
Journal volume	8
Journal issue	3
Pages of publication	854
a	9.1861 ± 0.0014 Å
b	11.669 ± 0.0018 Å
c	16.746 ± 0.003 Å
α	73.2 ± 0.003°
β	89.465 ± 0.003°
γ	77.158 ± 0.003°
Cell volume	1672.5 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.065
Residual factor for significantly intense reflections	0.0461
Weighted residual factors for significantly intense reflections	0.1239
Weighted residual factors for all reflections included in the refinement	0.1383
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179562 (current)	2016-03-24	cif/4/50/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/50/31.	4503109.cif
120110	2014-07-12	Adding DOIs to range 4/50 structures.	4503109.cif
41356	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4503109, 4503110, 4503111, 4503112, 4503113, 4503114 via cif-deposit CGI script.	4503109.cif