Crystallography Open Database

Information card for entry 4505654

Preview

Coordinates	4505654.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Ge H3 N O8 Sn6
Calculated formula	Ge H3 N O8 Sn6
Title of publication	Ammonothermal Crystal Growth of Germanium and Its Alloys: Synthesis of a Hollow Metallic Crystal
Authors of publication	Purdy, Andrew P.; Case, Sean; George, Clifford
Journal of publication	Crystal Growth & Design
Year of publication	2003
Journal volume	3
Journal issue	2
Pages of publication	121
a	10.4959 ± 0.0006 Å
b	10.4959 ± 0.0006 Å
c	10.4959 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	1156.27 ± 0.11 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	5
Space group number	196
Hermann-Mauguin space group symbol	F 2 3
Hall space group symbol	F 2 2 3
Residual factor for all reflections	0.055
Residual factor for significantly intense reflections	0.0535
Weighted residual factors for significantly intense reflections	0.1291
Weighted residual factors for all reflections included in the refinement	0.1299
Goodness-of-fit parameter for all reflections included in the refinement	1.148
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4505654.cif
120110	2014-07-12	Adding DOIs to range 4/50 structures.	4505654.cif
53679	2012-04-20	cif/ Adding structures of 4505652, 4505653, 4505654 via cif-deposit CGI script.	4505654.cif