Crystallography Open Database

Information card for entry 4507227

Preview

Coordinates	4507227.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Na24 Si136
Calculated formula	Na24 Si136
Title of publication	Pressure Effects on the Size of Type-I and Type-II Si-Clathrates Synthesized by Spark Plasma Sintering
Authors of publication	Stefanoski, S.; Blosser, M. C.; Nolas, G. S.
Journal of publication	Crystal Growth & Design
Year of publication	2013
Journal volume	13
Journal issue	1
Pages of publication	195
a	14.7156 ± 0.0001 Å
b	14.7156 ± 0.0001 Å
c	14.7156 ± 0.0001 Å
α	90°
β	90°
γ	90°
Cell volume	3186.65 ± 0.04 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	2
Space group number	227
Hermann-Mauguin space group symbol	F d -3 m :2
Hall space group symbol	-F 4vw 2vw 3
Residual factor for all reflections	0.0662
Residual factor for significantly intense reflections	0.063
Weighted residual factors for significantly intense reflections	0.0879
Weighted residual factors for all reflections included in the refinement	0.0885
Goodness-of-fit parameter for all reflections included in the refinement	1.577
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179608 (current)	2016-03-24	cif/4/50/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/50/72.	4507227.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4507227.cif
73859	2013-02-21	cif/ Adding structures of 4507227 via cif-deposit CGI script.	4507227.cif