Crystallography Open Database

Information card for entry 4509657

Preview

Coordinates	4509657.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H32 Cl Cu2 N8 O40 P W12
Calculated formula	C48 H32 Cl Cu2 N8 O40 P W12
Title of publication	Hydrothermal Syntheses, Crystal Structures, And Magnetic Properties of a Series of Complexes Constructed from Multinuclear Copper Clusters and Polyoxometalates
Authors of publication	Yang, Hongxun; Guo, Shengping; Tao, Jun; Lin, Jingxiang; Cao, Rong
Journal of publication	Crystal Growth & Design
Year of publication	2009
Journal volume	9
Journal issue	11
Pages of publication	4735
a	24.315 ± 0.005 Å
b	11.846 ± 0.002 Å
c	24.468 ± 0.004 Å
α	90°
β	97.635 ± 0.004°
γ	90°
Cell volume	6985 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0604
Residual factor for significantly intense reflections	0.0521
Weighted residual factors for significantly intense reflections	0.139
Weighted residual factors for all reflections included in the refinement	0.1568
Goodness-of-fit parameter for all reflections included in the refinement	1.149
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179632 (current)	2016-03-24	cif/4/50/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/50/96.	4509657.cif
97432	2014-01-29	cif/ Adding structures of 4509656, 4509657, 4509658, 4509659 via cif-deposit CGI script.	4509657.cif