Crystallography Open Database

Information card for entry 4518937

Preview

Coordinates	4518937.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H39 O7 P3 Rh2
Calculated formula	C34 H39 O7 P3 Rh2
Title of publication	Distinct Catalytic Performance of Dirhodium(II) Complexes with ortho-Metalated DPPP in Dehydrosilylation of Styrene Derivatives with Alkoxysilanes
Authors of publication	Lu, Wenkui; Zhu, Xiaoyu; Yang, Liqun; Wu, Xiaoyu; Xie, Xiaomin; Zhang, Zhaoguo
Journal of publication	ACS Catalysis
Year of publication	2021
Journal volume	11
Journal issue	16
Pages of publication	10190 - 10197
a	9.8701 ± 0.0002 Å
b	21.0572 ± 0.0004 Å
c	16.6273 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	3455.76 ± 0.11 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0284
Residual factor for significantly intense reflections	0.0238
Weighted residual factors for significantly intense reflections	0.0559
Weighted residual factors for all reflections included in the refinement	0.0576
Goodness-of-fit parameter for all reflections included in the refinement	1.106
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
268479 (current)	2021-09-04	cif/ Updating files of 4518936, 4518937 Original log message: Adding full bibliography for 4518936--4518937.cif.	4518937.cif
267894	2021-08-03	cif/ Adding structures of 4518937 via cif-deposit CGI script.	4518937.cif