Crystallography Open Database

Information card for entry 7000235

Preview

Coordinates	7000235.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C61 H78 N2 P4 Pt
Calculated formula	C61 H78 N2 P4 Pt
Title of publication	Reactions of R2P‒P(SiMe3)Li with [(R′3P)2PtCl2]. A general and efficient entry to phosphanylphosphinidene complexes of platinum. Syntheses and structures of [(η2-PPiPr2)Pt(p-Tol3P)2], [(η2-PPtBu2)Pt(p-Tol3P)2], [{η2-PP(NiPr2)2}Pt(p-Tol3P)2] and [{(Et2PhP)2Pt}2P2]
Authors of publication	Domańska-Babul, Wioleta; Chojnacki, Jaroslaw; Matern, Eberhard; Pikies, Jerzy
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	1
Pages of publication	146 - 151
a	15.336 ± 0.003 Å
b	24.002 ± 0.005 Å
c	18.974 ± 0.007 Å
α	90°
β	125.737 ± 0.019°
γ	90°
Cell volume	5669 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0396
Residual factor for significantly intense reflections	0.0346
Weighted residual factors for significantly intense reflections	0.0734
Weighted residual factors for all reflections included in the refinement	0.0752
Goodness-of-fit parameter for all reflections included in the refinement	1.107
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179680 (current)	2016-03-24	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/02.	7000235.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7000235.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7000235.cif
1143	2010-05-03	cif/7/ Adding CIFs from Dalton-Trans-2009/ deposition.	7000235.cif