Crystallography Open Database

Information card for entry 7003482

Preview

Coordinates	7003482.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C8 H24 Li N Si2 Zn
Calculated formula	C8 H23.397 Li N Si2 Zn
Title of publication	Synthesis and structural elucidation of solvent-free and solvated lithium dimethyl (HMDS) zincates
Authors of publication	Armstrong, David R.; Herd, Emma; Graham, David V.; Hevia, Eva; Kennedy, Alan R.; Clegg, William; Russo, Luca
Journal of publication	Dalton Transactions
Year of publication	2008
Journal issue	10
Pages of publication	1323 - 1330
a	6.784 ± 0.0003 Å
b	13.9936 ± 0.0007 Å
c	15.8133 ± 0.0007 Å
α	90°
β	97.65 ± 0.002°
γ	90°
Cell volume	1487.84 ± 0.12 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1045
Residual factor for significantly intense reflections	0.0655
Weighted residual factors for significantly intense reflections	0.1251
Weighted residual factors for all reflections included in the refinement	0.1347
Goodness-of-fit parameter for all reflections included in the refinement	1.239
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179738 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/34.	7003482.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7003482.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7003482.cif
1173	2010-05-16	cif/7/: adding data from Dalton-Trans-2008, New-J-Chem-2008, Org-Biomol-Chem-2008 and RSC-2008 processing.	7003482.cif