Crystallography Open Database

Information card for entry 7004152

Preview

Coordinates	7004152.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H60 Cl2 Mg2 N6 Si2
Calculated formula	C41 H60 Cl2 Mg2 N6 Si2
Title of publication	Magnesium amido N-heterocyclic carbene complexes
Authors of publication	Arnold, Polly L.; Edworthy, Ian S.; Carmichael, Christopher D.; Blake, Alexander J.; Wilson, Claire
Journal of publication	Dalton Transactions
Year of publication	2008
Journal issue	28
Pages of publication	3739 - 3746
a	16.2204 ± 0.0012 Å
b	9.3907 ± 0.0007 Å
c	31.198 ± 0.002 Å
α	90°
β	100.191 ± 0.002°
γ	90°
Cell volume	4677.1 ± 0.6 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0718
Residual factor for significantly intense reflections	0.048
Weighted residual factors for significantly intense reflections	0.112
Weighted residual factors for all reflections included in the refinement	0.122
Goodness-of-fit parameter for all reflections included in the refinement	0.94
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179745 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/41.	7004152.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7004152.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7004152.cif
1173	2010-05-16	cif/7/: adding data from Dalton-Trans-2008, New-J-Chem-2008, Org-Biomol-Chem-2008 and RSC-2008 processing.	7004152.cif