Crystallography Open Database

Information card for entry 7004540

Preview

Coordinates	7004540.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H23 Cl11 N4 Ru
Calculated formula	C25 H23 Cl11 N4 Ru
Title of publication	An easy electrochemical and chemical synthesis of [Ru(bpy)(CH3CN)2Cl2]: a synthon for heteroleptic tris(diimine) Ru(ii) complexes
Authors of publication	Chardon-Noblat, Sylvie; Renfrew, Anna; Lafolet, Frédéric; Deronzier, Alain; Jakonen, Minna; Laurila, Elina; Haukka, Matti
Journal of publication	Dalton Transactions
Year of publication	2008
Journal issue	43
Pages of publication	5891 - 5896
a	12.9977 ± 0.0007 Å
b	16.1554 ± 0.0009 Å
c	16.1347 ± 0.0006 Å
α	90°
β	92.813 ± 0.003°
γ	90°
Cell volume	3383.9 ± 0.3 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0687
Residual factor for significantly intense reflections	0.052
Weighted residual factors for significantly intense reflections	0.1291
Weighted residual factors for all reflections included in the refinement	0.1385
Goodness-of-fit parameter for all reflections included in the refinement	1.075
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179749 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/45.	7004540.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7004540.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7004540.cif
1173	2010-05-16	cif/7/: adding data from Dalton-Trans-2008, New-J-Chem-2008, Org-Biomol-Chem-2008 and RSC-2008 processing.	7004540.cif