Crystallography Open Database

Information card for entry 7005554

Preview

Coordinates	7005554.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H62 N3 Pb Si2
Calculated formula	C38 H62 N3 Pb Si2
Title of publication	Synthesis and theoretical studies on rare three-coordinate lead complexes.
Authors of publication	Chen, Matthew; Fulton, J. Robin; Hitchcock, Peter B.; Johnstone, Nick C.; Lappert, Michael F.; Protchenko, Andrey V.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	26
Pages of publication	2770 - 2778
a	11.9346 ± 0.0001 Å
b	13.3033 ± 0.0001 Å
c	14.6879 ± 0.0002 Å
α	97.37°
β	100.251 ± 0.001°
γ	115.65 ± 0.001°
Cell volume	2012.46 ± 0.04 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0289
Residual factor for significantly intense reflections	0.025
Weighted residual factors for significantly intense reflections	0.0562
Weighted residual factors for all reflections included in the refinement	0.0578
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179759 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/55.	7005554.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7005554.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7005554.cif
1186	2010-06-03	Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing.	7005554.cif