Crystallography Open Database

Information card for entry 7005678

Preview

Coordinates	7005678.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C130 H114 Br2 F12 Mn N6 O4 P8 W2
Calculated formula	C130 H114 Br2 F12 Mn N6 O4 P8 W2
Title of publication	Extended-chain, multinuclear transition metal complexes bridged by cyanodiazenido(1-), [N=N-C[triple bond, length as m-dash]N]-, ligands.
Authors of publication	Chan, Yun Fu; Chippindale, Ann M.; Colquhoun, Howard M.; Drew, Michael G. B.; Williams, David J.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	32
Pages of publication	3538 - 3545
a	12.3745 ± 0.0002 Å
b	16.1371 ± 0.0001 Å
c	18.3672 ± 0.0002 Å
α	66.321 ± 0.001°
β	77.507 ± 0.001°
γ	72.376 ± 0.001°
Cell volume	3182.37 ± 0.07 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0427
Residual factor for significantly intense reflections	0.0348
Weighted residual factors for significantly intense reflections	0.0905
Weighted residual factors for all reflections included in the refinement	0.0943
Goodness-of-fit parameter for all reflections included in the refinement	1.062
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179760 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/56.	7005678.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7005678.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7005678.cif
1186	2010-06-03	Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing.	7005678.cif