Crystallography Open Database

Information card for entry 7005791

Preview

Coordinates	7005791.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C150.5 H232 N4 O9 Sm3
Calculated formula	C150.5 H231.5 N4 O9 Sm3
Title of publication	Synthesis and structural characterization of novel mixed-valent samarium and divalent ytterbium and europium complexes supported by amine bis(phenolate) ligands.
Authors of publication	Guo, Huadong; Zhou, Hui; Yao, Yingming; Zhang, Yong; Shen, Qi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	32
Pages of publication	3555 - 3561
a	14.9171 ± 0.0004 Å
b	20.2284 ± 0.0003 Å
c	30.2896 ± 0.0006 Å
α	108.104 ± 0.009°
β	95.546 ± 0.01°
γ	104.692 ± 0.013°
Cell volume	8248.9 ± 0.9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1184
Residual factor for significantly intense reflections	0.0904
Weighted residual factors for significantly intense reflections	0.2139
Weighted residual factors for all reflections included in the refinement	0.2294
Goodness-of-fit parameter for all reflections included in the refinement	1.142
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	7005791.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7005791.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7005791.cif
1186	2010-06-03	Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing.	7005791.cif