Crystallography Open Database

Information card for entry 7006059

Preview

Coordinates	7006059.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H43.83 N8 O43.83 Sb6 V15
Calculated formula	C12 H42 N8 O43.8333 Sb6 V15
Title of publication	[V(IV)15Sb(III)6O42]6-: an antimony analogue of the molecular magnet [V15As6O42(H2O)]6-.
Authors of publication	Kiebach, Ragnar; Näther, Christian; Kögerler, Paul; Bensch, Wolfgang
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	30
Pages of publication	3221 - 3223
a	21.5209 ± 0.0009 Å
b	21.5209 ± 0.0009 Å
c	72.662 ± 0.004 Å
α	90°
β	90°
γ	120°
Cell volume	29145 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.0871
Residual factor for significantly intense reflections	0.06
Weighted residual factors for significantly intense reflections	0.1471
Weighted residual factors for all reflections included in the refinement	0.162
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179764 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/60.	7006059.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7006059.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7006059.cif
31985	2012-01-04	cif/ Canging data item '_diffrn_standards_decay_% none' to '_diffrn_standards_decay_% 0'.	7006059.cif
1186	2010-06-03	Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing.	7006059.cif