Crystallography Open Database

Information card for entry 7006252

Preview

Coordinates	7006252.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C132 H160 Br2 Cl4 N10 O26 P8 Rh2 W2
Calculated formula	C132 H136 Br2 Cl4 N10 O26 P8 Rh2 W2
Title of publication	The oxadiazolyldiazenido(1-) ligand: a remarkably versatile platform for the synthesis of heteropolynuclear transition metal complexes.
Authors of publication	Colquhoun, Howard M.; Chan, Yun Fu; Cardin, Christine J.; Drew, Michael G. B.; Gan, Yu; Abd El Kader, Kareem; White, Terence M.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	35
Pages of publication	3864 - 3867
a	14.2326 ± 0.0015 Å
b	26.598 ± 0.003 Å
c	21.292 ± 0.002 Å
α	90°
β	108.357 ± 0.01°
γ	90°
Cell volume	7650.1 ± 1.5 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	9
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1625
Residual factor for significantly intense reflections	0.0794
Weighted residual factors for significantly intense reflections	0.1939
Weighted residual factors for all reflections included in the refinement	0.233
Goodness-of-fit parameter for all reflections included in the refinement	1.007
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179766 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/62.	7006252.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7006252.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7006252.cif
1186	2010-06-03	Adding CIFs from Chem-Comm-2010_20-22/ and Dalton-Trans-2007/ processing.	7006252.cif