Crystallography Open Database

Information card for entry 7007113

Preview

Coordinates	7007113.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H20 F24 N5 O16 S8 Tm
Calculated formula	C17.004 H20 F24.012 N5 O16.008 S8.004 Tm
Title of publication	The first homoleptic bis(trifluoromethanesulfonyl)amide complex compounds of trivalent f-elements.
Authors of publication	Babai, Arash; Mudring, Anja-Verena
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2006
Journal issue	15
Pages of publication	1828 - 1830
a	20.1575 ± 0.0019 Å
b	14.8847 ± 0.0008 Å
c	16.1968 ± 0.0012 Å
α	90°
β	113.234 ± 0.006°
γ	90°
Cell volume	4465.5 ± 0.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	7
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/c 1
Hall space group symbol	-P 2yc
Residual factor for all reflections	0.1212
Residual factor for significantly intense reflections	0.0938
Weighted residual factors for significantly intense reflections	0.252
Weighted residual factors for all reflections included in the refinement	0.2796
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179775 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/71.	7007113.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7007113.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7007113.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7007113.cif