Crystallography Open Database

Information card for entry 7007221

Preview

Coordinates	7007221.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H78 I La N2 O P2
Calculated formula	C52 H78 I La N2 O P2
Title of publication	Amino-functionalised diarylphosphide complexes of the alkali metals and lanthanum.
Authors of publication	Izod, Keith; Liddle, Stephen T.; Clegg, William; Harrington, Ross W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2006
Journal issue	28
Pages of publication	3431 - 3437
a	11.8858 ± 0.0005 Å
b	13.2783 ± 0.0006 Å
c	18.7371 ± 0.0009 Å
α	74.358 ± 0.001°
β	86.267 ± 0.001°
γ	65.602 ± 0.001°
Cell volume	2589.7 ± 0.2 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.036
Residual factor for significantly intense reflections	0.031
Weighted residual factors for significantly intense reflections	0.0788
Weighted residual factors for all reflections included in the refinement	0.0815
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.6985 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179776 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/72.	7007221.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7007221.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7007221.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7007221.cif