Crystallography Open Database

Information card for entry 7007587

Preview

Coordinates	7007587.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C108 H99 Ag4 B4 F16 N27
Calculated formula	C108 H99 Ag4 B1.5 F6 N27
Title of publication	Complexes of Ag(I), Hg(I) and Hg(II) with multidentate pyrazolyl-pyridine ligands: From mononuclear complexes to coordination polymers via helicates, a mesocate, a cage and a catenate.
Authors of publication	Argent, Stephen P.; Adams, Harry; Riis-Johannessen, Thomas; Jeffery, John C.; Harding, Lindsay P.; Clegg, William; Harrington, Ross W.; Ward, Michael D.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2006
Journal issue	42
Pages of publication	4996 - 5013
a	16.281 ± 0.011 Å
b	18.3 ± 0.012 Å
c	23.28 ± 0.015 Å
α	72.91 ± 0.006°
β	78.379 ± 0.006°
γ	76.302 ± 0.006°
Cell volume	6376 ± 7 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1945
Residual factor for significantly intense reflections	0.1414
Weighted residual factors for significantly intense reflections	0.3683
Weighted residual factors for all reflections included in the refinement	0.3919
Goodness-of-fit parameter for all reflections included in the refinement	1.183
Diffraction radiation wavelength	0.6712 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179779 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/75.	7007587.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7007587.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7007587.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7007587.cif