Crystallography Open Database

Information card for entry 7008914

Preview

Coordinates	7008914.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H58 Li O5 Si2
Calculated formula	C47 H58 Li O5 Si2
Title of publication	A novel α,ω silyl dianionic salt. The synthesis and characterization of remotely connected benzannulated silole monoanions
Authors of publication	Choi, Seok-Bong; Boudjouk, Philip
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	6
Pages of publication	841
a	13.271 ± 0.0009 Å
b	13.9844 ± 0.0009 Å
c	14.0125 ± 0.0009 Å
α	64.636 ± 0.001°
β	77.45 ± 0.001°
γ	74.03 ± 0.001°
Cell volume	2244.3 ± 0.3 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1085
Residual factor for significantly intense reflections	0.0838
Weighted residual factors for significantly intense reflections	0.1967
Weighted residual factors for all reflections included in the refinement	0.2186
Goodness-of-fit parameter for all reflections included in the refinement	1.086
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179793 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/89.	7008914.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7008914.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7008914.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7008914.cif