Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7008980
Preview
| Coordinates | 7008980.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C36 H52 P2 Pd2 Si2 |
|---|---|
| Calculated formula | C36 H52 P2 Pd2 Si2 |
| SMILES | [P](CC)(CC)([Pd]123[H][Si]2(c2ccccc2)(c2ccccc2)[Pd]21([P](CC)(CC)CC)[H][Si]32(c1ccccc1)c1ccccc1)CC |
| Title of publication | Dipalladium complexes with bridging diorganosilyl ligands. Synthesis, structure, and properties of [LPd(μ-SiH(R)Ph)]2 (R = Ph or Me; L = PMe3, PEt3 or PMePh2) |
| Authors of publication | Kim, Yong-Joo; Lee, Sang-Chul; Park, Jong-Il; Osakada, Kohtaro; Choi, Jun-Chul; Yamamoto, Takakazu |
| Journal of publication | Journal of the Chemical Society, Dalton Transactions |
| Year of publication | 2000 |
| Journal issue | 3 |
| Pages of publication | 417 |
| a | 10.242 ± 0.009 Å |
| b | 11.447 ± 0.006 Å |
| c | 9.725 ± 0.008 Å |
| α | 112.13 ± 0.05° |
| β | 115.65 ± 0.06° |
| γ | 78.56 ± 0.06° |
| Cell volume | 951.2 ± 1.4 Å3 |
| Cell temperature | 296.2 K |
| Ambient diffraction temperature | 296.2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for significantly intense reflections | 0.038 |
| Weighted residual factors for all reflections included in the refinement | 0.045 |
| Goodness-of-fit parameter for all reflections included in the refinement | 2.57 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176453 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7. |
7008980.cif |
| 129439 | 2015-01-07 | cod/ (robertas@burundukas) Correcting values of _exptl_crystal_density_meas and _exptl_crystal_density_method data items: codsql "select codid from validation where message like '%\\'_exptl_crystal_density_meas\\' value \"not measured\" is %'" -NB \ | codid2file \ | xargs perl -i -pe "s/_exptl_crystal_density_meas\\s+'not +measured'/_exptl_crystal_density_meas ?/i; \ s/_exptl_crystal_density_method\\s+('not +measured'|\\?|none)/_exptl_crystal_density_method ./i" |
7008980.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7008980.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7008980.cif |
| 3896 | 2010-12-08 | cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/. |
7008980.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.