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Information card for entry 7009037
Preview
| Coordinates | 7009037.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | Tetrabromodi(μ-bisdiphenylstibinomethane)dipalladium(II).2dichloromethane |
|---|---|
| Formula | C52 H48 Br4 Cl4 Pd2 Sb4 |
| Calculated formula | C51.072 Br4 Cl2.144 Pd2 Sb4 |
| Title of publication | Synthesis, properties and structures of complexes of platinum metal halides and Group 11 metals with two distibinomethane ligands, R2SbCH2SbR2 (R = Me or Ph) |
| Authors of publication | Even, Tina; Genge, Anthony R. J.; Hill, Angela M.; Holmes, Nicholas J.; Levason, William; Webster, Michael |
| Journal of publication | Journal of the Chemical Society, Dalton Transactions |
| Year of publication | 2000 |
| Journal issue | 5 |
| Pages of publication | 655 |
| a | 15.953 ± 0.005 Å |
| b | 17 ± 0.004 Å |
| c | 11.943 ± 0.003 Å |
| α | 109.18 ± 0.02° |
| β | 109.95 ± 0.02° |
| γ | 79.65 ± 0.02° |
| Cell volume | 2867.2 ± 1.4 Å3 |
| Cell temperature | 150 K |
| Ambient diffraction temperature | 150 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0651 |
| Residual factor for significantly intense reflections | 0.0651 |
| Weighted residual factors for all reflections | 0.0762 |
| Weighted residual factors for all reflections included in the refinement | 0.0762 |
| Goodness-of-fit parameter for all reflections | 2.469 |
| Goodness-of-fit parameter for all reflections included in the refinement | 2.469 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179794 (current) | 2016-03-25 | cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/90. |
7009037.cif |
| 129439 | 2015-01-07 | cod/ (robertas@burundukas) Correcting values of _exptl_crystal_density_meas and _exptl_crystal_density_method data items: codsql "select codid from validation where message like '%\\'_exptl_crystal_density_meas\\' value \"not measured\" is %'" -NB \ | codid2file \ | xargs perl -i -pe "s/_exptl_crystal_density_meas\\s+'not +measured'/_exptl_crystal_density_meas ?/i; \ s/_exptl_crystal_density_method\\s+('not +measured'|\\?|none)/_exptl_crystal_density_method ./i" |
7009037.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7009037.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7009037.cif |
| 3896 | 2010-12-08 | cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/. |
7009037.cif |
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Users of the data should acknowledge the original authors of the
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