Crystallography Open Database

Information card for entry 7009144

Preview

Coordinates	7009144.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H34 Cl4 N2 O4 Pd
Calculated formula	C38 H34 Cl4 N2 O4 Pd
Title of publication	Binaphthyl Schiff base complexes of palladium(II). Structures and reactivities toward alkene epoxidation
Authors of publication	Zhou, Xiang-Ge; Huang, Jie-Sheng; Yu, Xiao-Qi; Zhou, Zhong-Yuan; Che, Chi-Ming
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	7
Pages of publication	1075
a	10.317 ± 0.002 Å
b	13.332 ± 0.003 Å
c	13.668 ± 0.003 Å
α	98.88 ± 0.03°
β	93.85 ± 0.03°
γ	102 ± 0.03°
Cell volume	1807.3 ± 0.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0876
Residual factor for significantly intense reflections	0.0788
Weighted residual factors for significantly intense reflections	0.1789
Weighted residual factors for all reflections included in the refinement	0.2344
Goodness-of-fit parameter for all reflections included in the refinement	1.28
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179795 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/91.	7009144.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009144.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009144.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009144.cif