Crystallography Open Database

Information card for entry 7009213

Preview

Coordinates	7009213.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H45 Bi N6 Si3
Calculated formula	C27 H45 Bi N6 Si3
SMILES	[Bi]123([n]4c(N1[Si](C)(C)C)cccc4C)([n]1c(N2[Si](C)(C)C)cccc1C)[n]1c(N3[Si](C)(C)C)cccc1C
Title of publication	Geminal arsa(III)amide and trisubstituted antimony and bismuth amides from the sterically hindered, N-functionalised amido ligand [{2-(6-Me)C5H3N}NSiMe3]−
Authors of publication	Raston, Colin L.; Skelton, Brian W.; Tolhurst, Vicki-Anne; White, Allan H.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	8
Pages of publication	1279
a	14.912 ± 0.005 Å
b	11.812 ± 0.004 Å
c	11.389 ± 0.004 Å
α	116.11 ± 0.02°
β	94.03 ± 0.03°
γ	104.73 ± 0.02°
Cell volume	1703.4 ± 1.1 Å³
Cell temperature	293 K
Ambient diffraction temperature	293 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.049
Residual factor for significantly intense reflections	0.038
Weighted residual factors for all reflections	0.039
Weighted residual factors for all reflections included in the refinement	0.038
Goodness-of-fit parameter for all reflections	1.392
Goodness-of-fit parameter for all reflections included in the refinement	1.45
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	7009213.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009213.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009213.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009213.cif