Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7009244
Preview
| Coordinates | 7009244.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | Complex of Bis(hexafluoroacetylacetonato)copper(II) with 4-(N-tert-Butyl-N-oxylamino)-2,2-bipyridine. |
|---|---|
| Formula | C24 H18 Cu F12 N3 O5 |
| Calculated formula | C24 H18 Cu F12 N3 O5 |
| Title of publication | Through-bond magnetic interaction between the 2p spin of the aminoxyl radical and the 3d spin of the metal ions in the complexes of bis(hexafluoroacetylacetonato)-manganese(II) and -copper(II) with 4-(N-tert-butyl-N-oxylamino)-2,2'-bipyridine † |
| Authors of publication | Kumada, Harumi; Sakane, Akira; Koga, Noboru; Iwamura, Hiizu |
| Journal of publication | Journal of the Chemical Society, Dalton Transactions |
| Year of publication | 2000 |
| Journal issue | 6 |
| Pages of publication | 911 |
| a | 8.496 ± 0.002 Å |
| b | 17.305 ± 0.003 Å |
| c | 20.1 ± 0.003 Å |
| α | 90° |
| β | 99.04 ± 0.02° |
| γ | 90° |
| Cell volume | 2918.5 ± 1 Å3 |
| Cell temperature | 296.2 K |
| Ambient diffraction temperature | 296.2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0563 |
| Residual factor for significantly intense reflections | 0.0563 |
| Weighted residual factors for significantly intense reflections | 0.0832 |
| Weighted residual factors for all reflections included in the refinement | 0.0832 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.924 |
| Diffraction radiation wavelength | 1.5418 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176453 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7. |
7009244.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7009244.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7009244.cif |
| 3896 | 2010-12-08 | cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/. |
7009244.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.