Crystallography Open Database

Information card for entry 7009256

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Coordinates	7009256.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	compound 13a
Formula	C28 H37 Cl2 Co N3 Ni O12 P3
Calculated formula	C28 H19 Cl2 Co N3 Ni O12 P3
Title of publication	An entry to half-sandwich complexes of first row transition metals (Ni, Co, Mn) containing the Kläui tripodal ligand, LOMe: synthesis and crystal structures of oligomeric, [LOMeM(μ-X)(L)]n (n = 2, 4), and monomeric complexes, LOMeM(L2)(X)
Authors of publication	De-qiang Ma; Shiro Hikichi; Munetaka Akita; Yoshihiko Moro-oka
Journal of publication	J. Chem. Soc., Dalton Trans.
Year of publication	2000
Journal issue	7
Pages of publication	1123 - 1134
a	19.733 ± 0.003 Å
b	18.211 ± 0.015 Å
c	20.147 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	7240 ± 6 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	8
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0932
Residual factor for significantly intense reflections	0.0764
Weighted residual factors for significantly intense reflections	0.1909
Weighted residual factors for all reflections included in the refinement	0.1984
Goodness-of-fit parameter for all reflections included in the refinement	1.327
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179796 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/92.	7009256.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009256.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009256.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009256.cif