Crystallography Open Database

Information card for entry 7009277

Preview

Coordinates	7009277.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H76 Mo2 N4 O6 Si4
Calculated formula	C64 H76 Mo2 N4 O6 Si4
Title of publication	High oxidation state imido metallasiloxanes: synthesis and structural characterisation of novel bis-imido chromium(VI) and molybdenum(VI) compounds †
Authors of publication	King, Lawrence; Motevalli, Majid; Sullivan, Alice C.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	8
Pages of publication	1357
a	12.395 ± 0.002 Å
b	15.831 ± 0.003 Å
c	17.246 ± 0.003 Å
α	90°
β	100.07 ± 0.03°
γ	90°
Cell volume	3332 ± 1.1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.2106
Residual factor for significantly intense reflections	0.0867
Weighted residual factors for significantly intense reflections	0.2059
Weighted residual factors for all reflections included in the refinement	0.2454
Goodness-of-fit parameter for all reflections included in the refinement	0.923
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179796 (current)	2016-03-25	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/92.	7009277.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7009277.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7009277.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7009277.cif