Crystallography Open Database

Information card for entry 7013949

Preview

Coordinates	7013949.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H60 Cu4 S4 Si4
Calculated formula	C24 H60 Cu4 S4 Si4
SMILES	[Cu]1[S]([Si](C)(C)C(C)(C)C)[Cu][S]([Si](C)(C)C(C)(C)C)[Cu][S]([Si](C)(C)C(C)(C)C)[Cu][S]1[Si](C)(C)C(C)(C)C
Title of publication	Synthesis and structural characterization of silanethiolato complexes having tert-butyldimethylsilyl and trimethylsilyl groups.
Authors of publication	Komuro, Takashi; Matsuo, Tsukasa; Kawaguchi, Hiroyuki; Tatsumi, Kazuyuki
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2004
Journal issue	10
Pages of publication	1618 - 1625
a	11.404 ± 0.004 Å
b	13.672 ± 0.005 Å
c	14.338 ± 0.005 Å
α	66.8 ± 0.01°
β	77.46 ± 0.02°
γ	86.71 ± 0.02°
Cell volume	2004.7 ± 1.3 Å³
Cell temperature	153.1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.046
Weighted residual factors for all reflections included in the refinement	0.104
Goodness-of-fit parameter for all reflections included in the refinement	1.015
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7013949.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7013949.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7013949.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7013949.cif