Crystallography Open Database

Information card for entry 7018403

Preview

Coordinates	7018403.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C53 H47 Cl9 P4 Pt
Calculated formula	C53 H47 Cl9 P4 Pt
Title of publication	Novel access to carbodiphosphoranes in the coordination sphere of group 10 metals: template synthesis and protonation of PCP pincer carbodiphosphorane complexes of C(dppm)(2).
Authors of publication	Reitsamer, Christian; Stallinger, Silvia; Schuh, Walter; Kopacka, Holger; Wurst, Klaus; Obendorf, Dagmar; Peringer, Paul
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	12
Pages of publication	3503 - 3514
a	9.4233 ± 0.0002 Å
b	15.0455 ± 0.0003 Å
c	19.0383 ± 0.0004 Å
α	90.021 ± 0.002°
β	90.644 ± 0.002°
γ	96.536 ± 0.002°
Cell volume	2681.5 ± 0.1 Å³
Cell temperature	233 ± 2 K
Ambient diffraction temperature	233 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0484
Residual factor for significantly intense reflections	0.0367
Weighted residual factors for significantly intense reflections	0.0678
Weighted residual factors for all reflections included in the refinement	0.0711
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179888 (current)	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/84.	7018403.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7018403.cif
52095	2012-04-07	../uploads/cif-deposit/cod/cif Adding structures of 7018399, 7018400, 7018401, 7018402, 7018403 via cif-deposit CGI script.	7018403.cif