Crystallography Open Database

Information card for entry 7019740

7019739 << 7019740 >> 7019741

Preview

Coordinates	7019740.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H116 Cl14 Co5 O62 Sb12
Calculated formula	C72 H48 Cl13.995 Co5 O62 Sb12
Title of publication	Isopolyoxometalates derived from arylstibonic acids with "reverse-Keggin ion" structures based on [M(RSb)(12)O(28)] cores, M = Co(ii) or Zn(ii).
Authors of publication	Nicholson, Brian K.; Clark, Christopher J.; Telfer, Shane G.; Groutso, Tania
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	33
Pages of publication	9964 - 9970
a	23.7522 ± 0.0003 Å
b	23.7522 ± 0.0003 Å
c	44.6195 ± 0.0015 Å
α	90°
β	90°
γ	120°
Cell volume	21800.3 ± 0.8 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	6
Space group number	155
Hermann-Mauguin space group symbol	R 3 2 :H
Hall space group symbol	R 3 2"
Residual factor for all reflections	0.0314
Residual factor for significantly intense reflections	0.0294
Weighted residual factors for significantly intense reflections	0.0826
Weighted residual factors for all reflections included in the refinement	0.0839
Goodness-of-fit parameter for all reflections included in the refinement	1.051
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179901 (current)	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/97.	7019740.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7019740.cif
64290	2012-08-12	cif/ Adding structures of 7019737, 7019738, 7019739, 7019740 via cif-deposit CGI script.	7019740.cif