Crystallography Open Database

Information card for entry 7022012

7022011 << 7022012 >> 7022013

Preview

Coordinates	7022012.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H70 Cl2 N2 O3 P4 Pd2 Te2
Calculated formula	C66 H64 Cl2 N2 O3 P4 Pd2 Te2
Title of publication	Reactivity of 2-chalcogenopyridines with palladium-phosphine complexes: isolation of different complexes depending on the nature of chalcogen atom and phosphine ligand.
Authors of publication	Chauhan, Rohit Singh; Kedarnath, G.; Wadawale, Amey; Slawin, Alexandra M. Z.; Jain, Vimal K.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	1
Pages of publication	259 - 269
a	11.934 ± 0.006 Å
b	13.083 ± 0.007 Å
c	13.46 ± 0.007 Å
α	114.084 ± 0.002°
β	99.385 ± 0.004°
γ	111.686 ± 0.005°
Cell volume	1656.3 ± 1.5 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0945
Residual factor for significantly intense reflections	0.0657
Weighted residual factors for significantly intense reflections	0.1577
Weighted residual factors for all reflections included in the refinement	0.1727
Goodness-of-fit parameter for all reflections included in the refinement	1.1
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179925 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/20.	7022012.cif
89945	2013-11-17	cif/ Adding structures of 7022012, 7022013, 7022014, 7022015 via cif-deposit CGI script.	7022012.cif