Crystallography Open Database

Information card for entry 7023639

Preview

Coordinates	7023639.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H51 F12 Ir N7 O P2 Rh
Calculated formula	C43 H49 F12 Ir N7 O P2 Rh
Title of publication	Comparison of ancillary ligand effects between 2,2'-bipyridine and 2-(2'-pyridyl)phenyl in the linkage and bridging isomerism of 5-methyltetrazolato iridium(III) and/or rhodium(III) complexes.
Authors of publication	Takayama, Asuka; Suzuki, Takayoshi; Ikeda, Miyu; Sunatsuki, Yukinari; Kojima, Masaaki
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	40
Pages of publication	14556 - 14567
a	26.1251 ± 0.001 Å
b	26.1251 ± 0.001 Å
c	14.4637 ± 0.0005 Å
α	90°
β	90°
γ	90°
Cell volume	9871.8 ± 0.6 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	8
Space group number	114
Hermann-Mauguin space group symbol	P -4 21 c
Hall space group symbol	P -4 2n
Residual factor for all reflections	0.0536
Residual factor for significantly intense reflections	0.0508
Weighted residual factors for significantly intense reflections	0.1371
Weighted residual factors for all reflections included in the refinement	0.1389
Goodness-of-fit parameter for all reflections included in the refinement	1.092
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179941 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/36.	7023639.cif
90592	2013-11-18	cif/ Adding structures of 7023631, 7023632, 7023633, 7023634, 7023635, 7023636, 7023637, 7023638, 7023639, 7023640, 7023641, 7023642 via cif-deposit CGI script.	7023639.cif