Crystallography Open Database

Information card for entry 7024402

Preview

Coordinates	7024402.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C50 H60 F6 N P2 Ru Sb Se
Calculated formula	C50 H60 F6 N P2 Ru Sb Se
Title of publication	Access to the first (iminophosphoranyl)(selenophosphoranyl)methane ligands Ph2P(=Se)CH2P(=NR)Ph2: coordination of their methanide and methandiide anions to ruthenium.
Authors of publication	Cadierno, Victorio; Díez, Josefina; García-Alvarez, Joaquín; Gimeno, José
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	3
Pages of publication	941 - 956
a	19.3086 ± 0.0002 Å
b	28.7968 ± 0.0003 Å
c	17.8805 ± 0.0002 Å
α	90°
β	100.455 ± 0.001°
γ	90°
Cell volume	9776.96 ± 0.18 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0654
Residual factor for significantly intense reflections	0.051
Weighted residual factors for significantly intense reflections	0.1368
Weighted residual factors for all reflections included in the refinement	0.1543
Goodness-of-fit parameter for all reflections included in the refinement	1.024
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179949 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/44.	7024402.cif
92472	2014-01-12	cif/ Adding structures of 7024401, 7024402, 7024403, 7024404, 7024405 via cif-deposit CGI script.	7024402.cif