Crystallography Open Database

Information card for entry 7024654

Preview

Coordinates	7024654.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H41 B F24 Ir N2 P
Calculated formula	C58 H41 B F24 Ir N2 P
Title of publication	Palladium and iridium complexes with a N,P,N-bis(pyridine)phenylphosphine ligand.
Authors of publication	Liu, Shaofeng; Peloso, Riccardo; Braunstein, Pierre
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	10
Pages of publication	2563 - 2572
a	12.5163 ± 0.0003 Å
b	14.9159 ± 0.0004 Å
c	16.5224 ± 0.0004 Å
α	85.787 ± 0.001°
β	77.882 ± 0.001°
γ	73.919 ± 0.001°
Cell volume	2897.47 ± 0.13 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0924
Residual factor for significantly intense reflections	0.0558
Weighted residual factors for significantly intense reflections	0.1342
Weighted residual factors for all reflections included in the refinement	0.1651
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179951 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/46.	7024654.cif
92612	2014-01-12	cif/ Adding structures of 7024649, 7024650, 7024651, 7024652, 7024653, 7024654, 7024655 via cif-deposit CGI script.	7024654.cif