Crystallography Open Database

Information card for entry 7024708

Preview

Coordinates	7024708.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H28 N P2 Se2 Tl
Calculated formula	C12 H28 N P2 Se2 Tl
Title of publication	Thallium(I) complexes of dichalcogenido imidodiphosphinates {Tl[(EP(i)Pr(2))(2)N]}(n) (E = Te, Se, S): Synthesis, NMR spectra and a structural comparison.
Authors of publication	Ritch, Jamie S.; Chivers, Tristram
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	7
Pages of publication	1745 - 1750
a	9.2446 ± 0.0018 Å
b	14.268 ± 0.003 Å
c	14.924 ± 0.003 Å
α	80.12 ± 0.03°
β	81.47 ± 0.03°
γ	84.22 ± 0.03°
Cell volume	1912.1 ± 0.7 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0485
Residual factor for significantly intense reflections	0.0372
Weighted residual factors for significantly intense reflections	0.0854
Weighted residual factors for all reflections included in the refinement	0.0925
Goodness-of-fit parameter for all reflections included in the refinement	1.084
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179952 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/47.	7024708.cif
92645	2014-01-12	cif/ Adding structures of 7024707, 7024708, 7024709 via cif-deposit CGI script.	7024708.cif