Crystallography Open Database

Information card for entry 7025479

Preview

Coordinates	7025479.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Tetrakis(tris(trimethylsilyl)germyl)distannene
Chemical name	Tetrakis[tris(trimethylsilyl)germyl]distannene
Formula	C18 H54 Ge2 Si6 Sn
Calculated formula	C18 H54 Ge2 Si6 Sn
Title of publication	EPR spectroscopic characterization of persistent germyl-substituted Pb(III)- and Sn(III)-radicals.
Authors of publication	Kurzbach, Dennis; Yao, Shenglai; Hinderberger, Dariush; Klinkhammer, Karl W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	28
Pages of publication	6449 - 6459
a	23.409 ± 0.006 Å
b	13.216 ± 0.004 Å
c	23.711 ± 0.007 Å
α	90°
β	106.6 ± 0.04°
γ	90°
Cell volume	7030 ± 4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	I 1 2/a 1
Hall space group symbol	-I 2ya
Residual factor for all reflections	0.0669
Residual factor for significantly intense reflections	0.036
Weighted residual factors for significantly intense reflections	0.0735
Weighted residual factors for all reflections included in the refinement	0.0817
Goodness-of-fit parameter for all reflections included in the refinement	0.861
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179960 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/54.	7025479.cif
93068	2014-01-12	cif/ Adding structures of 7025477, 7025478, 7025479, 7025480, 7025481, 7025482 via cif-deposit CGI script.	7025479.cif