Crystallography Open Database

Information card for entry 7026285

Preview

Coordinates	7026285.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H32 N P Zn
Calculated formula	C22 H32 N P Zn
SMILES	[Zn]1([P](C(C)C)(C(C)C)c2ccccc2N1c1c(C)cccc1C)CC
Title of publication	Amido phosphine complexes of zinc: synthesis, structure, and catalytic ring-opening polymerization of epsilon-caprolactone.
Authors of publication	Liang, Lan-Chang; Lee, Wei-Ying; Tsai, Tzung-Ling; Hsu, Yu-Lin; Lee, Ting-Yu
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	37
Pages of publication	8748 - 8758
a	8.621 ± 0.0002 Å
b	9.1959 ± 0.0002 Å
c	14.8726 ± 0.0004 Å
α	106.072 ± 0.001°
β	91.347 ± 0.001°
γ	106.942 ± 0.001°
Cell volume	1076.83 ± 0.05 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0437
Residual factor for significantly intense reflections	0.0344
Weighted residual factors for significantly intense reflections	0.0887
Weighted residual factors for all reflections included in the refinement	0.0949
Goodness-of-fit parameter for all reflections included in the refinement	1.099
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179968 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/62.	7026285.cif
93456	2014-01-13	cif/ Adding structures of 7026283, 7026284, 7026285, 7026286, 7026287, 7026288, 7026289 via cif-deposit CGI script.	7026285.cif