Crystallography Open Database

Information card for entry 7026430

Preview

Coordinates	7026430.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H58 Ni P2 Si5
Calculated formula	C22 H58 Ni P2 Si5
SMILES	[Si]1(C(CCC1([Si](C)(C)C)[Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C)=[Ni]([P](C)(C)C)[P](C)(C)C
Title of publication	Synthesis and structures of (dialkylsilylene)bis(phosphine)-nickel, palladium, and platinum complexes and (η(6)-arene)(dialkylsilylene)nickel complexes.
Authors of publication	Watanabe, Chieko; Inagawa, Yuichiro; Iwamoto, Takeaki; Kira, Mitsuo
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	39
Pages of publication	9414 - 9420
a	9.476 ± 0.003 Å
b	32.504 ± 0.009 Å
c	11.672 ± 0.003 Å
α	90°
β	112.327 ± 0.003°
γ	90°
Cell volume	3325.5 ± 1.6 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0568
Residual factor for significantly intense reflections	0.038
Weighted residual factors for significantly intense reflections	0.0839
Weighted residual factors for all reflections included in the refinement	0.0923
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179970 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/64.	7026430.cif
93497	2014-01-13	cif/ Adding structures of 7026430, 7026431, 7026432, 7026433 via cif-deposit CGI script.	7026430.cif