Crystallography Open Database

Information card for entry 7026713

Preview

Coordinates	7026713.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44.5 H47 Cl5 N2 O2 P4 Pt2
Calculated formula	C44 H47 Cl4 N2 O2 P4 Pt2
Title of publication	Transition metal chemistry of cyclodiphosphanes containing phosphine and amide-phosphine functionalities: formation of a stable dipalladium(II) complex containing a Pd-P σ-bond.
Authors of publication	Balakrishna, Maravanji S.; Venkateswaran, Ramalingam; Mague, Joel T.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	46
Pages of publication	11149 - 11162
a	10.109 ± 0.002 Å
b	25 ± 0.005 Å
c	10.463 ± 0.002 Å
α	90°
β	108.739 ± 0.002°
γ	90°
Cell volume	2504.1 ± 0.9 Å³
Cell temperature	220 ± 2 K
Ambient diffraction temperature	220 ± 2 K
Number of distinct elements	7
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0449
Residual factor for significantly intense reflections	0.038
Weighted residual factors for significantly intense reflections	0.0967
Weighted residual factors for all reflections included in the refinement	0.1004
Goodness-of-fit parameter for all reflections included in the refinement	1.067
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179973 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/67.	7026713.cif
93570	2014-01-13	cif/ Adding structures of 7026708, 7026709, 7026710, 7026711, 7026712, 7026713, 7026714, 7026715 via cif-deposit CGI script.	7026713.cif