Crystallography Open Database

Information card for entry 7035226

Preview

Coordinates	7035226.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C6 H16 N2 O6 P2 Pb
Calculated formula	C6 H16 N2 O6 P2 Pb
SMILES	C1C[P](C)(C)[Pb]([P]1(C)C)(ON(=O)=O)ON(=O)=O
Title of publication	Lead(ii) nitrate and hexafluorosilicate complexes with neutral diphosphine coordination.
Authors of publication	Burt, Jennifer; Grantham, William; Levason, William; Reid, Gillian
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	25
Pages of publication	11533 - 11541
a	8.2128 ± 0.0018 Å
b	8.2128 ± 0.0018 Å
c	20.989 ± 0.007 Å
α	90°
β	90°
γ	90°
Cell volume	1415.7 ± 0.6 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	92
Hermann-Mauguin space group symbol	P 41 21 2
Hall space group symbol	P 4abw 2nw
Residual factor for all reflections	0.0294
Residual factor for significantly intense reflections	0.0255
Weighted residual factors for significantly intense reflections	0.0554
Weighted residual factors for all reflections included in the refinement	0.0562
Goodness-of-fit parameter for all reflections included in the refinement	0.951
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	7035226.cif
143539	2015-07-11	cif/ Updating files of 7035226, 7035227, 7035228, 7035229, 7035230, 7035231 Original log message: Adding full bibliography for 7035226--7035231.cif.	7035226.cif
137180	2015-05-22	cif/ Adding structures of 7035226, 7035227, 7035228, 7035229, 7035230, 7035231 via cif-deposit CGI script.	7035226.cif