Crystallography Open Database

Information card for entry 7036778

Preview

Coordinates	7036778.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H53 N2 Nb O2 P3
Calculated formula	C43 H53 N2 Nb O2 P3
Title of publication	Assembly and stabilization of {E(cyclo-P3)2} (E = Sn, Pb) as a bridging ligand spanning two triaryloxyniobium units.
Authors of publication	Velian, Alexandra; Cossairt, Brandi M.; Cummins, Christopher C.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	5
Pages of publication	1891 - 1895
a	14.0102 ± 0.001 Å
b	16.5289 ± 0.0012 Å
c	18.0957 ± 0.001 Å
α	90°
β	92.662 ± 0.004°
γ	90°
Cell volume	4186 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0554
Residual factor for significantly intense reflections	0.0388
Weighted residual factors for significantly intense reflections	0.0923
Weighted residual factors for all reflections included in the refinement	0.1013
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176068 (current)	2016-02-05	cif/ Updating files of 7036776, 7036777, 7036778, 7036779, 7036780, 7036781 Original log message: Adding full bibliography for 7036776--7036781.cif.	7036778.cif
160979	2015-10-08	cif/ Adding structures of 7036776, 7036777, 7036778, 7036779, 7036780, 7036781 via cif-deposit CGI script.	7036778.cif