Crystallography Open Database

Information card for entry 7040091

Preview

Coordinates	7040091.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H29 F6 N O2 Rh S Sb
Calculated formula	C21 H29 F6 N O2 Rh S Sb
Title of publication	Half-sandwich complexes of rhodium containing cysteine-derived ligands.
Authors of publication	Carmona, María; Rodríguez, Ricardo; Lahoz, Fernando J.; García-Orduña, Pilar; Osante, Iñaki; Cativiela, Carlos; López, José A; Carmona, Daniel
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	36
Pages of publication	14203 - 14215
a	12.326 ± 0.003 Å
b	11.038 ± 0.003 Å
c	19.034 ± 0.005 Å
α	90°
β	103.541 ± 0.004°
γ	90°
Cell volume	2517.7 ± 1.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	8
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0885
Residual factor for significantly intense reflections	0.0606
Weighted residual factors for significantly intense reflections	0.1136
Weighted residual factors for all reflections included in the refinement	0.1269
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
187111 (current)	2016-10-08	cif/ Updating files of 7040089, 7040090, 7040091, 7040092 Original log message: Adding full bibliography for 7040089--7040092.cif.	7040091.cif
184773	2016-08-02	cif/ Adding structures of 7040089, 7040090, 7040091, 7040092 via cif-deposit CGI script.	7040091.cif