Crystallography Open Database

Information card for entry 7041627

Preview

Coordinates	7041627.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H39 F Si Sn3
Calculated formula	C33 H39 F Si Sn3
SMILES	[Sn](C#Cc1c([Si](F)(c2ccccc2C#C[Sn](C)(C)C)c2ccccc2C#C[Sn](C)(C)C)cccc1)(C)(C)C
Title of publication	Tridentate Lewis-acids based on triphenylsilane.
Authors of publication	Tomaschautzky, Janek; Neumann, Beate; Stammler, Hans-Georg; Mix, Andreas; Mitzel, Norbert W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2017
Journal volume	46
Journal issue	5
Pages of publication	1645 - 1659
a	12.80666 ± 0.00009 Å
b	41.3809 ± 0.0002 Å
c	13.17067 ± 0.00013 Å
α	90°
β	90.2126 ± 0.0007°
γ	90°
Cell volume	6979.76 ± 0.09 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100 ± 0.1 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0394
Residual factor for significantly intense reflections	0.0376
Weighted residual factors for significantly intense reflections	0.0937
Weighted residual factors for all reflections included in the refinement	0.0955
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
191654 (current)	2017-02-04	cif/ Updating files of 7041624, 7041625, 7041626, 7041627, 7041628, 7041629, 7041630, 7041631, 7041632, 7041633, 7041634, 7041635, 7041636, 7041637, 7041638, 7041639, 7041640 Original log message: Adding full bibliography for 7041624--7041640.cif.	7041627.cif
190007	2017-01-07	cif/ Adding structures of 7041624, 7041625, 7041626, 7041627, 7041628, 7041629, 7041630, 7041631, 7041632, 7041633, 7041634, 7041635, 7041636, 7041637, 7041638, 7041639, 7041640 via cif-deposit CGI script.	7041627.cif