Crystallography Open Database

Information card for entry 7046279

Preview

Coordinates	7046279.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C106 H150 Cl6 F18 N10 O22 Rh4 S6
Calculated formula	C106 H150 Cl6 F18 N10 O22 Rh4 S6
Title of publication	Construction of half-sandwich multinuclear complexes including tunnel architectures via C-H-activation-directed assembly.
Authors of publication	Guo, Bei-Bei; Gao, Wen-Xi; Lin, Yue-Jian; Jin, Guo-Xin
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	23
Pages of publication	7701 - 7708
a	14.5885 ± 0.0005 Å
b	25.624 ± 0.0009 Å
c	17.9554 ± 0.0007 Å
α	90°
β	91.106 ± 0.002°
γ	90°
Cell volume	6710.8 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1131
Residual factor for significantly intense reflections	0.0865
Weighted residual factors for significantly intense reflections	0.2241
Weighted residual factors for all reflections included in the refinement	0.2473
Goodness-of-fit parameter for all reflections included in the refinement	1.014
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
229886 (current)	2019-11-17	cif/ Updating files of 7046278, 7046279, 7046280, 7046281, 7046282 Original log message: Adding full bibliography for 7046278--7046282.cif.	7046279.cif
207702	2018-05-09	cif/ Adding structures of 7046278, 7046279, 7046280, 7046281, 7046282 via cif-deposit CGI script.	7046279.cif