Crystallography Open Database

Information card for entry 7048270

Preview

Coordinates	7048270.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	H10 N4 S4 W
Calculated formula	H10 N4 S4 W
Title of publication	Nanostructured tungsten sulfides: insights into precursor decomposition and the microstructure using X-ray scattering methods.
Authors of publication	Mangelsen, Sebastian; Srinivasan, Bikshandarkoil R.; Schürmann, Ulrich; Kienle, Lorenz; Näther, Christian; Bensch, Wolfgang
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	4
Pages of publication	1184 - 1201
a	6.6033 ± 0.0008 Å
b	7.4965 ± 0.0008 Å
c	18.663 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	923.8 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0233
Residual factor for significantly intense reflections	0.0186
Weighted residual factors for significantly intense reflections	0.0431
Weighted residual factors for all reflections included in the refinement	0.0442
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
224077 (current)	2019-11-07	cif/ Updating files of 7048270, 7048271 Original log message: Adding full bibliography for 7048270--7048271.cif.	7048270.cif
212246	2018-11-30	cif/ Adding structures of 7048270, 7048271 via cif-deposit CGI script.	7048270.cif