Crystallography Open Database

Information card for entry 7048530

Preview

Coordinates	7048530.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Mg{(tBu2pz)2CHSiMe2NiPr}({N(SiMe3)2}
Formula	C37 H68 Mg N6 Si3
Calculated formula	C37 H68 Mg N6 Si3
Title of publication	Magnesium, calcium and zinc [N<sub>2</sub>N'] heteroscorpionate complexes.
Authors of publication	Luna Barros, Mariana; Cushion, Michael G.; Schwarz, Andrew D.; Turner, Zoë R; Mountford, Philip
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	13
Pages of publication	4124 - 4138
a	13.9372 ± 0.0002 Å
b	15.275 ± 0.0002 Å
c	20.1552 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	4290.86 ± 0.09 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	5
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0461
Residual factor for significantly intense reflections	0.0357
Weighted residual factors for all reflections	0.0421
Weighted residual factors for significantly intense reflections	0.0372
Weighted residual factors for all reflections included in the refinement	0.0372
Goodness-of-fit parameter for all reflections included in the refinement	1.1189
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
224283 (current)	2019-11-08	cif/ Updating files of 7048527, 7048528, 7048529, 7048530, 7048531, 7048532, 7048533, 7048534, 7048535, 7048536, 7048537, 7048538 Original log message: Adding full bibliography for 7048527--7048538.cif.	7048530.cif
212959	2019-01-11	cif/ Adding structures of 7048527, 7048528, 7048529, 7048530, 7048531, 7048532, 7048533, 7048534, 7048535, 7048536, 7048537, 7048538 via cif-deposit CGI script.	7048530.cif