Crystallography Open Database

Information card for entry 7049008

Preview

Coordinates	7049008.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H46 Ni P2 Si4
Calculated formula	C26 H46 Ni P2 Si4
Title of publication	Isolation of two bis(silyl)nickel complexes with Si-Si bond formation in a single-crystal-to-single-crystal fashion.
Authors of publication	Zhang, Sen-Yu; Li, Jie; Zhao, Sheng-Ze; Wang, Shi; Lu, Min-Ming; Li, Yong-Hua; Huang, Wei
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	10
Pages of publication	3433 - 3439
a	12.4689 ± 0.0008 Å
b	12.4689 ± 0.0008 Å
c	20.552 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	3195.3 ± 0.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	116
Hermann-Mauguin space group symbol	P -4 c 2
Hall space group symbol	P -4 -2c
Residual factor for all reflections	0.0326
Residual factor for significantly intense reflections	0.0256
Weighted residual factors for significantly intense reflections	0.0535
Weighted residual factors for all reflections included in the refinement	0.0542
Goodness-of-fit parameter for all reflections included in the refinement	0.891
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
223812 (current)	2019-11-07	cif/ Updating files of 7049008, 7049009 Original log message: Adding full bibliography for 7049008--7049009.cif.	7049008.cif
213631	2019-02-14	cif/ Adding structures of 7049008, 7049009 via cif-deposit CGI script.	7049008.cif