Crystallography Open Database

Information card for entry 7059554

Preview

Coordinates	7059554.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H44 Cl2 N4 O2 Pb Se2
Calculated formula	C32 H44 Cl2 N4 O2 Pb Se2
Title of publication	Acylselenoureato bis(chelates) of lead: synthesis, structural characterization and microwave-assisted formation of PbSe nano- and microstructures
Authors of publication	Klauke, Karsten; Schmitz, Alexa; Swertz, Ann-Christin; Beele, Björn B.; Giesen, Beatriz; Schlüsener, Carsten; Janiak, Christoph; Mohr, Fabian
Journal of publication	New Journal of Chemistry
Year of publication	2020
Journal volume	44
Journal issue	19
Pages of publication	7719 - 7726
a	17.9384 ± 0.0005 Å
b	19.0184 ± 0.0012 Å
c	10.4156 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	3553.4 ± 0.3 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	7
Space group number	45
Hermann-Mauguin space group symbol	I b a 2
Hall space group symbol	I 2 -2c
Residual factor for all reflections	0.0299
Residual factor for significantly intense reflections	0.0238
Weighted residual factors for significantly intense reflections	0.0465
Weighted residual factors for all reflections included in the refinement	0.0489
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
257769 (current)	2020-10-06	cif/ Updating files of 7059550, 7059551, 7059552, 7059553, 7059554 Original log message: Adding full bibliography for 7059550--7059554.cif.	7059554.cif
252866	2020-06-05	cif/ Updating files of 7059550, 7059551, 7059552, 7059553, 7059554 Original log message: Adding full bibliography for 7059550--7059554.cif.	7059554.cif
251346	2020-05-01	cif/ Adding structures of 7059550, 7059551, 7059552, 7059553, 7059554 via cif-deposit CGI script.	7059554.cif