Crystallography Open Database

Information card for entry 7059732

Preview

Coordinates	7059732.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	(AsPh4)4[(WO2)4(9HL)4].4MeOH.4H2O
Formula	C152 H124 As4 O36 W4
Calculated formula	C150 H108 As4 O30 W4
Title of publication	A new fluorone-based bridging ligand for discrete and polymeric assemblies including Mo and W based [4+4] metallocycles
Authors of publication	Sutton, Ashley L.; Abrahams, Brendan F.; Hudson, Timothy A.; Robson, Richard
Journal of publication	New Journal of Chemistry
Year of publication	2020
Journal volume	44
Journal issue	27
Pages of publication	11437 - 11440
a	30.3905 ± 0.0003 Å
b	30.3905 ± 0.0003 Å
c	14.8757 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	13738.9 ± 0.3 Å³
Cell temperature	130.15 K
Ambient diffraction temperature	130.15 K
Number of distinct elements	5
Space group number	92
Hermann-Mauguin space group symbol	P 41 21 2
Hall space group symbol	P 4abw 2nw
Residual factor for all reflections	0.0467
Residual factor for significantly intense reflections	0.0428
Weighted residual factors for significantly intense reflections	0.0964
Weighted residual factors for all reflections included in the refinement	0.098
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
257678 (current)	2020-10-06	cif/ Updating files of 7059731, 7059732, 7059733, 7059734 Original log message: Adding full bibliography for 7059731--7059734.cif.	7059732.cif
255057	2020-08-06	cif/ Updating files of 7059731, 7059732, 7059733, 7059734 Original log message: Adding full bibliography for 7059731--7059734.cif.	7059732.cif
253548	2020-06-30	cif/ Adding structures of 7059731, 7059732, 7059733, 7059734 via cif-deposit CGI script.	7059732.cif